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Further purification of adduct (10/26/1976 - 10/27/1976)

Purpose/Intro: "I will take the fractions checked above and concentrate them down to remove most of the MeOH. Then, if all goes well, put the concentrate through the preparative column."
Results/Conclusion: "The adduct probably is in the precipitate. It consists of white crystals that are needle-like in shape."
Notes: Sample 10-26-1 is the pooled fractions. Solid materials precipitated during rotary evaporation. The supernatant is 10-26-2; the insoluble material is 10-26-3.

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