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Preparation of a pure, dry adduct sample (11/28/1976)

Purpose/Intro: "Sample 11-3-2 is good-quality adduct and some small portions have been used in HCl-stability studies by Paul Donahue. I want some dry adduct as a backup sample for the NMR to be run in D2O/DCl."
Notes: Sample 11-28-1

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