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Obtain UV spectrum of "Diol" peak from adduct methylation experiment (02/05/1977)
Purpose/Intro: "The data reported on previous page imply that 3-MeGua may have been present in the "diol" peak. If this peak is a diol, it should undergo a bathochromic shift in alkali, like B2α."
Results/Conclusion: "In alkaline solution, no bathochromic shift was observed. The UV at pH 6 looked similar to adduct (high A264/A360). The data indicate that the "diol" peak probably is a derivative of the adduct and not a breakdown product."
Notes: Note the control sample; the authentic diol.
Links:
PDF: See this in the notebook!
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